艾附暖宫胶囊挥发油提取及包合工艺

祁秀玲; 曹德英; 王晓琦; 王静; 付秀英

doi:10.13422/j.cnki.syfjx.2012.09.065

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艾附暖宫胶囊挥发油提取及包合工艺

工艺与制剂 | 更新时间：2024-09-23

- 艾附暖宫胶囊挥发油提取及包合工艺
- Extraction and Inclusion Technology of Volatile Oil from Aifu Nuangong Capsule
- 中国实验方剂学杂志 2012年18卷第9期页码：53-56
- 作者机构：
  
  1. 沧州医学高等专科学校
  2. 河北医科大学
  3. 沧州市药检所
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2012.09.065
  中图分类号： R283
- 纸质出版日期：2012
- 稿件说明：
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[1]祁秀玲,曹德英,王晓琦,王静,付秀英.艾附暖宫胶囊挥发油提取及包合工艺[J].中国实验方剂学杂志,2012,18(09):53-56.

QI Xiu-ling1, CAO De-ying2, WANG Xiao-qi3, et al. Extraction and Inclusion Technology of Volatile Oil from Aifu Nuangong Capsule[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(9): 53-56.
[1]祁秀玲,曹德英,王晓琦,王静,付秀英.艾附暖宫胶囊挥发油提取及包合工艺[J].中国实验方剂学杂志,2012,18(09):53-56. DOI： 10.13422/j.cnki.syfjx.2012.09.065.

QI Xiu-ling1, CAO De-ying2, WANG Xiao-qi3, et al. Extraction and Inclusion Technology of Volatile Oil from Aifu Nuangong Capsule[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(9): 53-56. DOI： 10.13422/j.cnki.syfjx.2012.09.065.

摘要

目的:优选艾附暖宫胶囊中挥发油的提取及包合工艺。方法:以浸泡时间、提取时间、加水倍数为考察因素

挥发油收率为指标

正交试验优选挥发油提取工艺;以挥发油和β-CD比例、包合温度和包合时间为考察因素

以包合物收率和包合率的综合评分为指标

正交试验优选挥发油包合工艺

并对包合物进行鉴别。结果:优选提取工艺为浸泡1 h

加8倍量水

提取7 h;优选包合工艺为β-CD-挥发油8∶1

包合温度50℃

包合时间1.0 h。结论:优选的提取及包合工艺可行、收率高、适合大生产。

Abstract

Objective:To optimize extraction and inclusion technology of volatile oil from Aifu Nuangong capsule.Method:With soaking time

extraction time and the amount of water as investigating factors

yield of volatile oil as index

orthogonal test was used to optimize extraction technology of volatile oil.With ratio of volatile oil-cyclodextrin

inclusion temperature and inclusion time as investigating factors

composite score of inclusion yield and inclusion ratio as index

orthogonal test was used to optimize inclusion technology of volatile oil

and inclusion compound was identified.Result:Optimized extraction technology was:powder was soaked 1 h with 8 times the amount of water

extracted 7 h.Optimized inclusion technology was:ratio of β-CD and volatile oil was 8∶ 1

inclusion temperature was 50 ℃

inclusion time was 1.0 h.Conclusion:This optimized technology was feasible with high yield

it could be suitable for large-scale production.

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