血栓心脉宁片挥发油化学成分的GC-MS分析

刘金平; 明磊; 刘海宇; 张庆贺; 林美妤; 刘传贵; 李平亚; 卢丹

doi:10.13422/j.cnki.syfjx.2012.15.038

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血栓心脉宁片挥发油化学成分的GC-MS分析

化学与分析 | 更新时间：2024-09-23

- 血栓心脉宁片挥发油化学成分的GC-MS分析
- Chemical Costituents in Volatile Oil from Xueshuan Xinmaining Tablet with GC-MS Analysis
- 中国实验方剂学杂志 2012年18卷第15期页码：93-95
- 作者机构：
  
  吉林大学再生医学科学研究所
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2012.15.038
  中图分类号： R286.0
- 纸质出版日期：2012
- 稿件说明：
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[1]刘金平,明磊,刘海宇,张庆贺,林美妤,刘传贵,李平亚,卢丹.血栓心脉宁片挥发油化学成分的GC-MS分析[J].中国实验方剂学杂志,2012,18(15):93-95.

LIU Jin-ping, MING Lei, LIU Hai-yu, et al. Chemical Costituents in Volatile Oil from Xueshuan Xinmaining Tablet with GC-MS Analysis[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(15): 93-95.
[1]刘金平,明磊,刘海宇,张庆贺,林美妤,刘传贵,李平亚,卢丹.血栓心脉宁片挥发油化学成分的GC-MS分析[J].中国实验方剂学杂志,2012,18(15):93-95. DOI： 10.13422/j.cnki.syfjx.2012.15.038.

LIU Jin-ping, MING Lei, LIU Hai-yu, et al. Chemical Costituents in Volatile Oil from Xueshuan Xinmaining Tablet with GC-MS Analysis[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(15): 93-95. DOI： 10.13422/j.cnki.syfjx.2012.15.038.

摘要

目的:分析比较不同批次血栓心脉宁片挥发油化学成分。方法:采用水蒸气蒸馏法提取挥发油

应用GC-MS分析鉴定了血栓心脉宁片挥发油的化学成分

面积归一化法测定其相对含量。结果:从批号110603药品中分离得到42个色谱峰

鉴定了其中36个化合物

主要成分为龙脑（43.25%）、异龙脑（30.03%）及麝香酮（7.95%）。从批号110309药品中分离得到40个色谱峰

鉴定了其中33个化合物

主要成分为龙脑（43.37%）、异龙脑（30.14%）及麝香酮（7.71%）。结论:两个批次的血栓心脉宁片挥发油化学成分基本一致

表明该药性质稳定。该方法简便、快速、重复性好

为血栓心脉宁片质量评价提供了一定的科学依据。

Abstract

Objective: To analyze the chemical constituents of volatile oil extracted from Xueshuan Xinmaining tablet.Method: Volatile oil was extracted by water-steam distillation.The components were quantitatively determined with normalization method

and were identified by GC-MS.Results: Forty-two compounds were separated by GC from batch of 110603 and 36 of them were identified.The major components were borneol（43.25%）

isoborneol（30.03%）and muscone（7.95%）.40 compounds were separated by GC from 110309 and 33 of them were identified.The major components were borneol（43.37%）

isoborneol（30.14%）and muscone（7.71%）.Conclusion: The chemical components in volatile oils were basically same in two samples

so the medicine is stable.The method is simple and rapid with good repeatability.It will provide theoretical foundation for its quality evaluation and clinical medication.

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