响应面法优化松花粉总酚的超声提取工艺

卢奕; 马力

doi:10.13422/j.cnki.syfjx.2012.16.068

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响应面法优化松花粉总酚的超声提取工艺

工艺与制剂 | 更新时间：2024-09-23

- 响应面法优化松花粉总酚的超声提取工艺
- Optimization of Ultrasonic-assisted Extraction Technology for Total Phenols from Pinus massoniana by Response Surface Methodology
- 中国实验方剂学杂志 2012年18卷第16期页码：53-56
- 作者机构：
  
  深圳市孙逸仙心血管医院
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2012.16.068
  中图分类号： R284.1
- 纸质出版日期：2012
- 稿件说明：
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[1]卢奕,马力.响应面法优化松花粉总酚的超声提取工艺[J].中国实验方剂学杂志,2012,18(16):53-56.

LU Yi, MA Li. Optimization of Ultrasonic-assisted Extraction Technology for Total Phenols from Pinus massoniana by Response Surface Methodology[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(16): 53-56.
[1]卢奕,马力.响应面法优化松花粉总酚的超声提取工艺[J].中国实验方剂学杂志,2012,18(16):53-56. DOI： 10.13422/j.cnki.syfjx.2012.16.068.

LU Yi, MA Li. Optimization of Ultrasonic-assisted Extraction Technology for Total Phenols from Pinus massoniana by Response Surface Methodology[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(16): 53-56. DOI： 10.13422/j.cnki.syfjx.2012.16.068.

摘要

目的:优选松花粉中总酚的超声提取工艺。方法:以总酚得率为指标

采用单因素试验考察乙醇体积分数、超声时间、超声温度、料液比等因素对总酚得率的影响

在此基础上

运用响应面法优选总酚超声提取工艺。结果:松花粉总酚的最佳超声提取工艺条件为30倍量39%乙醇于51℃下超声提取24 min

在此条件下

总酚得率3.85 mg.g-1

实测值与模型预测值相符。结论:响应面分析法可较好地用于优化松花粉总酚超声提取工艺

且该优选工艺方便、快捷、高效。

Abstract

Objective:To optimize ultrasonic-assisted extraction technology of total phenols from Pinus massoniana by response surface methodology.Method: With yield of total phenols as index

the concentration of ethanol

ultrasonic time

ultrasonic temperature and solid-liquid ratio were investigated by single factor test

based on this

ultrasonic extraction technology of total phenols was optimized by response surface methodology.Result: Optimal extraction conditions were:ultrasonic extracted 24 min with 30 times the amount of 39% ethanol at 51 ℃

under these conditions

yield of total phenols reached 3.85 mg · g-1

which was agreed with model predictions.Conclusion: Ultrasonic-assisted extraction technology was simple

rapid

and efficient

response surface method could used well to optimize ultrasonic-assisted extraction of total phenols from P.massoniana.

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