ZHAO Yong-hui. Determination of Stachydrine Hydrochloride in Yimucao Soft Capsule by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(5): 142-144.
ZHAO Yong-hui. Determination of Stachydrine Hydrochloride in Yimucao Soft Capsule by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(5): 142-144. DOI: 10.13422/j.cnki.syfjx.2013.05.063.
HPLC测定益母草软胶囊中盐酸水苏碱的含量
摘要
目的:应用高效液相色谱法测定益母草软胶囊中盐酸水苏碱的含量。方法:采用Kromasi C18(4.6 mm×250 mm
Objective:An HPLC method was established for determination of stachydrine hydrochloride in Yimucao Soft Capsule.Method: Chromatographic column was Kromasi-C18 with acetonitrile-water(80∶20) as the mobile phase.The detection wavelength was set at 192 nm and flow rate was 1.0 mL·min-1.Result: Stachydrine hydrochloride was separated with a good linearity in the sample size ranges of 2.456-12.280 μg.The average recovery was 98.67%
with RSD 1.39%.Conclusion: The method is simple
specific and reproducible to control the quality of Yimucao Capsule.