TONG Hong, TANG Jun. Analysis of Volatile Components from Lavender by Three Different Methods[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(16): 100-105.
TONG Hong, TANG Jun. Analysis of Volatile Components from Lavender by Three Different Methods[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(16): 100-105. DOI: 10.13422/j.cnki.syfjx.2014160100.
Objective: The study aimed to compare the difference of volatile components in lavender by different extraction methods. Method: Volatile components from lavender were extracted by steam distillation (SDE)
microwave extraction (MWE)
head space-solid phase microextraction (HS-SPME) respectively
and analyzed by gas chromatography-mass spectrometry (GC-MS). Result: There was a certain difference among the volatile compounds extracted by the above three methods. Totally
54 volatile components were identified
including 17 alcohols
11 alkenes
11 esters
3 ketones
2 aldehydes
and 10 other components such as phenols
amines
caryophyllene oxide and so on. Among the detected compounds in the samples
34 terpenoids with pharmacological activity were identified
and 7 common compounds were identified by three methods
namely α-terpinene
linalool oxide
linalool
linalyl acetate
cryptone
(Z)-β-farnesene and caryophyllene oxide. Characteristic components were specific to each extraction method:hotrienol
nerol
nerolidol
cuminol
α-cedrol and camphor were characteristic components from SDE method; α-santalene
germacrene
tau-cadinol
pichtosin
α-epoxy-terpenyl acetate and three other compounds were the characteristic components by MWE method; 8-acetoxy linalool
1-hydroxy linalool
butyric acid-3-hexenyl ester
limonene oxide
3
16-diacetyl pseudo solasodine and thirteen other compounds were the main characteristic components via HS-SPME method. Conclusion: The above three methods combined with GC-MS can be used for the analysis of different volatile compounds in lavender and thus be feasible to establish GC-MS representation system for it.