PENG Liu, ZHOU Jun, FAN Kai-jing. Determination of Mangifer in Ermu Ningsou Wan by an Indirect Flame Atomic Absorption Spectrometry[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(1): 95-98.
PENG Liu, ZHOU Jun, FAN Kai-jing. Determination of Mangifer in Ermu Ningsou Wan by an Indirect Flame Atomic Absorption Spectrometry[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(1): 95-98. DOI: 10.13422/j.cnki.syfjx.2015010095.
Objective: To establish an indirect atomic absorption spectrometry method for determination content of mangifer in Ermu Ningsou Wan. Method: Based on the mangifer can be quantitatively generate brown precipitation with Sr2+ in alkaline environment
the content of mangifer in samples was determined indirectly by atomic absorption spectrometry. The effects of temperature
reaction time
pH value and amount of strontium chloride were studied. Result: The conditions of precipitate reaction were chosen as follow:1.00 mL strontium chloride solutions (1.395 g·L-1)
40℃
pH 9.0
and react 20 minutes. Meanwhile
the linear range was 2.11 to 59.95 mg·L-1 and the detection limit was 0.25 mg·L-1. The recovery rate was 96.74%±1.07%. This method performed good stability
precision and repeatability. Conclusion: The proposed method is easy to control and allows the determination of mangifer in a wide range. The results for the analysis are satisfactory.