麝香舒活灵的渗漉提取工艺优选

崔龙; 卢鹏; 曹丽华; 尚强; 曹晖; 高进

doi:10.13422/j.cnki.syfjx.2015200041

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麝香舒活灵的渗漉提取工艺优选

药剂与炮制 | 更新时间：2024-01-04

- 麝香舒活灵的渗漉提取工艺优选
- Optimization of Percolation Extraction Process of Shexiang Shuhuoling
- 中国实验方剂学杂志 2015年21卷第20期页码：41-43
- 作者机构：
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- DOI：10.13422/j.cnki.syfjx.2015200041
  中图分类号： R284.2
- 纸质出版日期：2015
- 稿件说明：
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崔龙, 卢鹏, 曹丽华, 等. 麝香舒活灵的渗漉提取工艺优选[J]. 中国实验方剂学杂志, 2015,21(20):41-43.

CUI Long, LU Peng, CAO Li-hua, et al. Optimization of Percolation Extraction Process of Shexiang Shuhuoling[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(20): 41-43.
崔龙, 卢鹏, 曹丽华, 等. 麝香舒活灵的渗漉提取工艺优选[J]. 中国实验方剂学杂志, 2015,21(20):41-43. DOI： 10.13422/j.cnki.syfjx.2015200041.

CUI Long, LU Peng, CAO Li-hua, et al. Optimization of Percolation Extraction Process of Shexiang Shuhuoling[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(20): 41-43. DOI： 10.13422/j.cnki.syfjx.2015200041.

摘要

目的:优选麝香舒活灵的渗漉提取工艺

为该制剂的工业化生产工艺改进提供参考。方法:在单因素试验基础上

以梓醇转移率及含固量为综合评价指标

乙醇体积分数、乙醇用量、渗漉速度、药材浸渍时间为考察因素

采用L9(34)正交试验优选麝香舒活灵的渗漉提取工艺。结果:最佳提取工艺条件为加15倍量50%乙醇浸渍6 h

流速0.25 mL·min-1。羟基红花黄色素A和梓醇的转移率分别为97.50%

102.07%

RSD分别为5.4%

3.5%。结论:该工艺提取率及有效成分转移率高

简单易行

适合麝香舒活灵的工业化大生产。

Abstract

Objective: To optimize percolation extraction process of Shexiang Shuhuoling

and provide a reference for process improvement of this preparation in industrial production. Method: Based on single factor test

with composite score of transferring rate of catalpol and solid-containing content as index

orthogonal experimental design was adopted to optimize percolation extraction process by taking percolation rate

immersion time

ethanol concentration and amount as factors. Result: Optimum percolation extraction process was added 15 times the amount of 50% ethanol for immersing 6 h

percolation rate of 0.25 mL·min-1.Transferring rates of hydroxy safflower yellow A and catalpol were 97.50% and 102.07% with RSD of 5.4% and 3.5%

respectively. Conclusion: This process is feasible and economical

which is suitable for industrial production of Shexiang Shuhuoling.

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