益气固脱颗粒质量标准

杨炳火; 谈瑄忠; 郎永英

doi:10.13422/j.cnki.syfjx.2015210070

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益气固脱颗粒质量标准

化学与分析 | 更新时间：2024-01-04

- 益气固脱颗粒质量标准
- Quality Standard of Compound Yiqi Gutuo Granules
- 中国实验方剂学杂志 2015年21卷第21期页码：70-73
- 作者机构：
- 作者简介：
- 基金信息：
  
  南京市医学科技发展专项(3601027)
- DOI：10.13422/j.cnki.syfjx.2015210070
  中图分类号： R286.0
- 纸质出版日期：2015
- 稿件说明：
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杨炳火, 谈瑄忠, 郎永英. 益气固脱颗粒质量标准[J]. 中国实验方剂学杂志, 2015,21(21):70-73.

YANG Bing-huo, TAN Xuan-zhong, LANG Yong-ying. Quality Standard of Compound Yiqi Gutuo Granules[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(21): 70-73.
杨炳火, 谈瑄忠, 郎永英. 益气固脱颗粒质量标准[J]. 中国实验方剂学杂志, 2015,21(21):70-73. DOI： 10.13422/j.cnki.syfjx.2015210070.

YANG Bing-huo, TAN Xuan-zhong, LANG Yong-ying. Quality Standard of Compound Yiqi Gutuo Granules[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(21): 70-73. DOI： 10.13422/j.cnki.syfjx.2015210070.

摘要

目的: 建立益气固脱颗粒的质量标准。方法: 采用薄层色谱(TLC)法对方中的黄芪、当归、枳壳进行定性鉴别

用HPLC对黄芪甲苷、阿魏酸进行含量测定。结果: TLC斑点清晰

分离度良好

阴性对照无干扰;黄芪甲苷、阿魏酸分别在0.112 0~1.120

0.012 0~0.120 g·L-1与峰面积积分值呈良好的线性关系

平均回收率依次为98.54%

97.79%

RSD分别为2.2%

1.9%。结论: 定性定量方法简便、结果准确可靠、专属性强

所建标准可用于益气固脱颗粒的质量控制。

Abstract

Objective: To establish the quality standard of Yiqi Gutuo granules. Method: Qualitative identification of Astragalus

Angelica and Citrus Aurantium in the formula was carried out by thin-layer chromatography (TLC). HPLC method was used for the determination of astragaloside and ferulic acid contents. Result: TLC spots were clear and well-separated without negative interference. The linear range of calycosin glucoside

ferulic acid were 0.012 0-0.120 and 0.112 0-1.120 g·L-1

respectively

with good linear relationship with the peak area integral value. The average recoveries were 98.54% and 97.79%

respectively. RSD were 2.2% and 1.9%

respectively. Conclusion: The qualitative and quantitative method is simple

convenient

accurate and reliable with good precision. It can be used for the quality control of Yiqi Gutuo granules.

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