毛血藤挥发性成分GC-MS分析

杨胜勇; 朱梦如; 张洁; 陆宽; 高玉琼

doi:10.13422/j.cnki.syfjx.2015240048

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毛血藤挥发性成分GC-MS分析

化学与分析 | 更新时间：2024-09-23

- 毛血藤挥发性成分GC-MS分析
- GC-MS Analysis of Volatile Constituents of
- 中国实验方剂学杂志 2015年21卷第24期页码：48-51
- 作者机构：
- 作者简介：
- 基金信息：
  
  贵州省省长专项资金项目[黔省专合字(2006)81号]
- DOI：10.13422/j.cnki.syfjx.2015240048
  中图分类号： O657.63;R284.1
- 纸质出版日期：2015
- 稿件说明：
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杨胜勇, 朱梦如, 张洁, 等. 毛血藤挥发性成分GC-MS分析[J]. 中国实验方剂学杂志, 2015,21(24):48-51.

YANG Sheng-yong, ZHU Meng-ru, ZHANG Jie, et al. GC-MS Analysis of Volatile Constituents of [J]. Chinese journal of experimental traditional medical formulae, 2015, 21(24): 48-51.
杨胜勇, 朱梦如, 张洁, 等. 毛血藤挥发性成分GC-MS分析[J]. 中国实验方剂学杂志, 2015,21(24):48-51. DOI： 10.13422/j.cnki.syfjx.2015240048.

YANG Sheng-yong, ZHU Meng-ru, ZHANG Jie, et al. GC-MS Analysis of Volatile Constituents of [J]. Chinese journal of experimental traditional medical formulae, 2015, 21(24): 48-51. DOI： 10.13422/j.cnki.syfjx.2015240048.

摘要

目的:分析毛血藤根茎的挥发性成分

为毛血藤的开发利用提供实验依据。方法:利用水蒸气蒸馏法提取毛血藤根茎的挥发性成分

采用气相色谱-质谱联用(GC-MS)技术对挥发性成分进行分析。结果:共分离出99个化学成分

鉴别出60个化学成分

占挥发油总量的68.598%

其主要成分为柏木脑(7.001%)

麝香草酚(5.948%)

己醛(4.593%)

双戊烯(3.708%)

芳姜黄酮(3.438%)

壬醛(3.256%)等。结论:本文采用气相色谱-质谱联用法对毛血藤根茎的挥发性成分进行研究

为毛血藤的综合利用提供科学依据。

Abstract

Objective: To provide the foundation for reasonable utilization by analyzing the volatile constituents of the rhizome of Polygonum cynanchoides. Method: The volatile constituents were extracted from the rhizome of P. cynanchoides by steam distillation. The chemical constituents were analyzed by gas chromatography-mass spectrography(GC-MS). Result: A total of 99 compounds were separated and 60 of them were identified

which accounted for 68.598% of the total volatile oil. The major components were cedrol(7.001%)

thymol(5.948%)

hexanal(4.593%)

dipentene(3.708%)

ar-tumerone(3.438%) and 1-nonanal(3.256%). Conclusion: This paper has studied the volatile constituents of the rhizome of P. cynanchoides using GC-MS

and provides a scientific basis for the comprehensive utilization of P. cynanchoides.

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