枳壳挥发油提取工艺优选及其化学成分GC-MS分析

张金莲; 刘明贵; 钟凌云; 颜冬梅; 龚千锋; 谢日健; 祝婧; 刘艳菊; 李娜

doi:10.13422/j.cnki.syfjx.2016190027

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枳壳挥发油提取工艺优选及其化学成分GC-MS分析

饮片工艺与质量研究专题 | 更新时间：2024-01-04

- 枳壳挥发油提取工艺优选及其化学成分GC-MS分析
- Optimization of Extraction Process of Volatile Oil from Aurantii Fructus and GC-MS Analysis of Its Chemical Constituents
- 中国实验方剂学杂志 2016年22卷第19期页码：27-31
- 作者机构：
- 作者简介：
- 基金信息：
  
  国家自然科学基金项目（81560651）;国家中医药管理局公益性科研专项（201507002-2）
- DOI：10.13422/j.cnki.syfjx.2016190027
  中图分类号： R284;O657.63
- 纸质出版日期：2016
- 稿件说明：
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张金莲, 刘明贵, 钟凌云, 等. 枳壳挥发油提取工艺优选及其化学成分GC-MS分析[J]. 中国实验方剂学杂志, 2016,22(19):27-31.

ZHANG Jin-lian, LIU Ming-gui, ZHONG Ling-yun, et al. Optimization of Extraction Process of Volatile Oil from Aurantii Fructus and GC-MS Analysis of Its Chemical Constituents[J]. Chinese journal of experimental traditional medical formulae, 2016, 22(19): 27-31.
张金莲, 刘明贵, 钟凌云, 等. 枳壳挥发油提取工艺优选及其化学成分GC-MS分析[J]. 中国实验方剂学杂志, 2016,22(19):27-31. DOI： 10.13422/j.cnki.syfjx.2016190027.

ZHANG Jin-lian, LIU Ming-gui, ZHONG Ling-yun, et al. Optimization of Extraction Process of Volatile Oil from Aurantii Fructus and GC-MS Analysis of Its Chemical Constituents[J]. Chinese journal of experimental traditional medical formulae, 2016, 22(19): 27-31. DOI： 10.13422/j.cnki.syfjx.2016190027.

摘要

目的：优选水蒸气蒸馏法提取枳壳挥发油的工艺，分析粉碎度对枳壳挥发油化学成分的影响。方法：采用正交试验确定水蒸气蒸馏法提取枳壳挥发油的工艺条件，以挥发油提取率为评价指标，粉碎度、加水量、浸泡时间、提取时间为考察因素。采用GC-MS对枳壳粉碎度为24目和50目所提取的挥发油进行化学成分鉴定。结果：最佳水蒸气蒸馏法工艺条件为枳壳粉碎度24目，加11倍量水浸泡0.5 h，提取7 h。从24目枳壳粉末挥发油中鉴定出45个组分，50目中鉴定出39个组分，分别占其挥发油总量的99.46%和99.53%。结论：优化的提取工艺重复性好、挥发油提取率较高且成分种类多，适用于枳壳挥发油的提取。

Abstract

Objective: To optimize extraction process of volatile oil from Aurantii Fructus

and analyze difference of chemical constituents in volatile oil from Aurantii Fructus with grinding degree of 24 mesh and 50 mesh. Method: Volatile oil from Aurantii Fructus was extracted by steam distillation

orthogonal test was adopted to optimize process of volatile oil.GC-MS was employed to compare similarities and differences between volatile oil from Aurantii Fructus with grinding degree of 24 mesh and 50 mesh. Result: Optimum extraction conditions of steam distillation were as follows:the comminution degree of 24 mesh

soaked 0.5 h and extracted 7 h with 11 times the amount of water.Forty-five components in volatile oil from Aurantii Fructus with grinding degree of 24 mesh were identified

there were 39 components for 50 mesh

accounting for 99.46%and 99.53%of total content of volatile oil

respectively. Conclusion: This optimized process is stable and feasible with high extraction rate of volatile oil.

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