ZHANG Xiao-fei, ZHAN Juan-juan, WU Si-qi, et al. Optimization of Extraction Technology of Volatile Oil from Angelicae Sinensis Radix and Analysis of Chemical Components in Its Aromatic Water[J]. Chinese journal of experimental traditional medical formulae, 2017, 23(5): 27-31.
ZHANG Xiao-fei, ZHAN Juan-juan, WU Si-qi, et al. Optimization of Extraction Technology of Volatile Oil from Angelicae Sinensis Radix and Analysis of Chemical Components in Its Aromatic Water[J]. Chinese journal of experimental traditional medical formulae, 2017, 23(5): 27-31. DOI: 10.13422/j.cnki.syfjx.2017050027.
Objective: To optimize the extraction process of volatile oil from Angelicae Sinensis Radix and fit its extraction kinetic model equation
and then to detect chemical components in volatile oil and aromatic water.Method: The improved extractor of volatile oil was adopted
extraction process of volatile oil from Angelicae Sinensis Radix was optimized by response surface methodology
then the extraction rate of volatile oil was fitted and the regression equations were calculated.Components in light oil
heavy oil and emulsified aromatic water during the extraction process of volatile oil were determined by GC-MS
in order to find out the chemical material base for formation of emulsification.Result: Optimal extraction process was as follows:extracting time of 8.55 h
solid-liquid ratio of 1:10
soaked 1.82 h;extraction rate of volatile oil was(0.70±0.01)%.Kinetic equations of optimal technology were V=0.72(1-e-0.000 74t) (R2=0.996 7) and ln(0.72-V)=-0.014 1t-0.349 3(R2=0.998 7).Components in aromatic water were different from those in volatile oil from Angelicae Sinensis Radix
especially for 2-vinyl-4-methoxyphenol.Conclusion: This optimized extraction process is feasible and stable
two extraction dynamics equations can be fitted to its extraction process
components in aromatic water have a larger difference with those in volatile oil.