LUO Jian-rong, XIAO Huai, ZHANG Cheng-gui, et al. Analysis on Oil Components in Two Kinds of Medicinal Blattaria by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2017, 23(11): 55-58.
LUO Jian-rong, XIAO Huai, ZHANG Cheng-gui, et al. Analysis on Oil Components in Two Kinds of Medicinal Blattaria by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2017, 23(11): 55-58. DOI: 10.13422/j.cnki.syfjx.2017110055.
Objective: To analyze chemical ingredients of oils from Periplaneta australasiae and P. americana
in order to provide experimental basis for reasonable utilization of animal medicines of blattaria. Method: Ethanol reflux extraction method was used to extract medicinal materials of blattaria
and petroleum ether was used to extract fat-soluble components. Its oil components were analyzed by GC-MS technique and identified by NIST11.L standard mass spectra library. HP-5MS fused-silica capillary column was adopted
the carrier gas was high-purity helium
electron impact ionization source was at 230 ℃
and quality scanning range was between m/z 12-550.Their relative contents were calculated by area normalization. Result: Thirty-seven compounds were identified in the oil of P. australasiae
accounting for 90.99% of the total weight. The compounds with higher content level included linoleic acid (29.86%)
oleic acid (26.30%)
hexacosane (10.57%)
stearic acid (3.94%)
and heptadecane (3.78%). Besides
a small amount of arachidonic acid was found in the oil of P. australasiae. Thirty-five compounds were identified in the oil of P. americana
accounting for 94.14% of the total weight. The compounds with higher content level included oleic acid (44.09%)
palmitic acid (16.03%)
stearic acid (6.32%)
and 3-eicosyne (5.31%). Conclusion: Esters
fatty acids and hydrocarbon compounds were the main compounds in the oils of P. australasiae and P. americana
but there were varying degrees of differences in the varieties and relative content. Totally 21 common constituents were identified in the oils from the two kinds of cockroaches
but there were great differences in the relative content.