4种不同药材来源郁金饮片中挥发油成分的GC-MS分析

张军; 王亮; 石典花; 王雪梅; 杜以琳; 孙立立

doi:10.13422/j.cnki.syfjx.2017130001

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4种不同药材来源郁金饮片中挥发油成分的GC-MS分析

药剂与炮制 | 更新时间：2024-01-04

- 4种不同药材来源郁金饮片中挥发油成分的GC-MS分析
- Analysis of Volatile Oil in Curcumae Radix Pieces from Four Different Sources by GC-MS
- 中国实验方剂学杂志 2017年23卷第13期页码：1-7
- 作者机构：
- 作者简介：
- 基金信息：
  
  国家自然科学基金项目（81503255）;山东省中医药科技发展计划项目（2013-115）
- DOI：10.13422/j.cnki.syfjx.2017130001
  中图分类号： O657.63;R284.1
- 纸质出版日期：2017
- 稿件说明：
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张军, 王亮, 石典花, 等. 4种不同药材来源郁金饮片中挥发油成分的GC-MS分析[J]. 中国实验方剂学杂志, 2017,23(13):1-7.

ZHANG Jun, WANG Liang, SHI Dian-hua, et al. Analysis of Volatile Oil in Curcumae Radix Pieces from Four Different Sources by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2017, 23(13): 1-7.
张军, 王亮, 石典花, 等. 4种不同药材来源郁金饮片中挥发油成分的GC-MS分析[J]. 中国实验方剂学杂志, 2017,23(13):1-7. DOI： 10.13422/j.cnki.syfjx.2017130001.

ZHANG Jun, WANG Liang, SHI Dian-hua, et al. Analysis of Volatile Oil in Curcumae Radix Pieces from Four Different Sources by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2017, 23(13): 1-7. DOI： 10.13422/j.cnki.syfjx.2017130001.

摘要

目的：分析4种不同药材来源郁金饮片中挥发油成分，找出其共有及差异成分，为该饮片的合理使用提供依据。方法：采用水蒸气蒸馏法提取挥发油，利用GC-MS对4种不同药材来源郁金饮片挥发油成分进行测定，载气高纯度氦气，进样温度250 ℃，压力49.5 kPa，总流量36.0 mL·min-1，柱流量1.0 mL·min-1，线速度36.1 cm·s-1；电离方式电子轰击离子源，电离电压70 eV，离子源温度200 ℃，接口温度280 ℃，溶剂延时3.5 min，m/z 40~400。结果：4种不同来源郁金饮片挥发油均检测出了50种成分，其中有3种共有成分，3种郁金共有成分达13种，2种郁金共有成分达15种；4种郁金共有、交互存在的挥发油成分达31种。结论：4种不同药材来源郁金饮片挥发油中存在共有及交互存在的成分。吉马酮可作为温郁金、桂郁金、绿丝郁金的含量测定指标成分；姜黄素、姜黄酮、芳姜黄酮等可作为黄丝郁金的含量测定指标成分。

Abstract

Objective: To analyze volatile oil in Curcumae Radix pieces from four different sources and find out the common and different components. Method: The volatile oil in Curcumae Radix pieces from four different sources were extracted by steam distillation and determined by GC-MS

carrier gas was helium

temperature was rose by program

ionization mode was electron bombardment ion source. Result: Fifty components were determined in volatile oil in Curcumae Radix pieces from four different sources and three common components were found in four Curcumae Radix pieces;thirteen common components were found in three Curcumae Radix pieces;fifteen common components were found in two Curcumae Radix pieces;thirty-one components were found in two or more Curcuma Radix pieces

and the proportion was 62%. Conclusion: Curcumae Radix pieces from four different sources have common and interactive components in volatile oil.

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