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纸质出版日期:2017
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刘颖, 苏桂云, 芦海生, 等. 不同部位三七粉显微特征及质量标准[J]. 中国实验方剂学杂志, 2017,23(23):34-39.
LIU Ying, SU Gui-yun, LU Hai-sheng, et al. Microscopic Characters and Quality Standards of Powder from Different Medicinal Parts[J]. Chinese journal of experimental traditional medical formulae, 2017, 23(23): 34-39.
刘颖, 苏桂云, 芦海生, 等. 不同部位三七粉显微特征及质量标准[J]. 中国实验方剂学杂志, 2017,23(23):34-39. DOI: 10.13422/j.cnki.syfjx.2017230034.
LIU Ying, SU Gui-yun, LU Hai-sheng, et al. Microscopic Characters and Quality Standards of Powder from Different Medicinal Parts[J]. Chinese journal of experimental traditional medical formulae, 2017, 23(23): 34-39. DOI: 10.13422/j.cnki.syfjx.2017230034.
目的:建立三七主根、剪口、筋条不同部位加工成的三七粉质量标准。方法:采用感官、色度测定、显微、理化、含量测定检验方法。结果:不同药用部位加工成的三七粉在外观颜色、显微特征、灰分、含量测定几个方面有明显区别,感官和显微特征不能区分三七的商品规格。颜色可以区分三七主根、剪口和筋条制成的三七粉,主根加工成的三七粉颜色最浅,呈黄白色,剪口与筋条加工成的三七粉颜色略深,呈现棕黄色和浅棕色,使用色差仪并结果经过SPSS分析结果与观察一致,剪口的颜色最深,筋条次之,主根颜色最浅;显微特征能够区分剪口和主根、筋条加工成的三七粉,剪口加工成的三七粉中可见纤维,主根与筋条加工成的三七粉中均未检出有纤维,剪口可见簇晶,主根中簇晶未检出;主根灰分全部合格,剪口和筋条有部分不合格,酸不溶性灰分全部合格。测定三七不同部位人参皂苷Rg1,人参皂苷Rb1及三七皂苷R1的含量,主根和筋条与剪口成分有明显差异。结论:颜色差异、显微特征区别、灰分数据、人参皂苷Rg1,人参皂苷Rb1及三七皂苷R1的含量为三七粉提供质量依据。
Objective: To provide quality basis for the Panax notoginseng powder processed from different parts. Method: Sensory
colorimetric method
microscopic
physical and chemical
and content determination methods were used in this study. Result: The P. notoginseng powder processed from different medicinal parts showed significant difference in appearance color
microscopic characteristics
ash content and content determination
sensory and microscopic characteristics can't be used to distinguish the P. notoginseng commodity specifications. Color can be used to distinguish the powder made of main root
notch and tendons
as the powder made of the main root showed the most shallow color
which was yellow and white
while the powder made of notch and tendons showed slightly deeper color
which was brownish yellow and light brown. The results were consistent with colorimeter observations based on SPSS analysis
which showed that cut the color was deepest in notch
followed by tendons
and the main root had the most shallow color. Microscopic features can be used to distinguish the powder made of notch and the main root
the tendons. The powder made of notch showed fibers
which were not detected in the main root and the tendons; clustered crystal was not detected in main root
but appeared in the notch; the ash content was all qualified in main root
but some were not qualified in notch and tendons; acid insoluble ash content was all qualified. The contents of ginsenoside Rg1
ginsenoside Rb1 and notoginsenoside R1 in different parts of P. notoginseng were significantly different. Conclusion: The color difference
microscopic characters
ash content
and ginsenoside Rg1
ginsenoside Rb1 and notoginsenoside R1 contents can provide quality basis for Panax notoginseng powder.
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