CHEN Xiang-sheng, LIU Yan-ju, CHEN Hai-xia, et al. Comparison of GC Fingerprints of Atractylodis Rhizoma Before and After Being Deep-fried[J]. Chinese journal of experimental traditional medical formulae, 2018, 24(2): 24-28.
CHEN Xiang-sheng, LIU Yan-ju, CHEN Hai-xia, et al. Comparison of GC Fingerprints of Atractylodis Rhizoma Before and After Being Deep-fried[J]. Chinese journal of experimental traditional medical formulae, 2018, 24(2): 24-28. DOI: 10.13422/j.cnki.syfjx.2018020024.
Objective:To establish GC fingerprints about volatile oil in the raw and deep-fired Atractylodis Rhizoma
and to clarify the changing rule of chemical compositions in volatile oil about Atractylodis Rhizoma before and after being deep-fried. Method:Volatile oil was extracted by steam distillation
and GC fingerprints of volatile oil in Atractylodis Rhizoma before and after being deep-fried were analyzed. Result:There were 25 common peaks in GC fingerprints of volatile oil in raw and processed products of Atractylodis Rhizoma
the relative retention time of these peaks was almost the same
but their relative peak areas changed significantly.For example
peaks areas of 15th
16th
17th
19th
23th
24th and 25th were reduced >20%.In GC fingerprints
the area ratio of peak 16 to 17 was greater than 3 in the raw products
but it was less than 3 in processed products;at the same time
the area ratio of peak 19 to 23 was less than 3 in the raw products
but it was greater than 3 in processed products. Conclusion:Difference of GC characteristic peaks in raw and processed products of Atractylodis Rhizoma is significant
and the results are stable with good specificity.It can be used as qualitative identification for Atractylodis Rhizoma between raw and processed products;as well as
it can lay foundation to interpretate the dropping dry and reduce the toxicity of Atractylodis Rhizoma after being deep-fried.