4种根茎类中药材在简易库和冷藏库中的理化指标分析

吴翠; 马玉翠; 洪专; 晋文慧; 徐靓; 巢志茂

doi:10.13422/j.cnki.syfjx.20180808

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4种根茎类中药材在简易库和冷藏库中的理化指标分析

化学与分析 | 更新时间：2024-01-04

- 4种根茎类中药材在简易库和冷藏库中的理化指标分析
- Analysis on Physiochemical Indexes of Four Kinds of Rhizome Chinese Medicinal Herbs Stored in Simple and Cool Warehouses
- 中国实验方剂学杂志 2018年24卷第8期页码：60-64
- 作者机构：
- 作者简介：
- 基金信息：
  
  国家中医药行业科研专项（201407005）;现代农业产业技术体系建设专项资金资助（CARS-21）
- DOI：10.13422/j.cnki.syfjx.20180808
  中图分类号： R284.1
- 纸质出版日期：2018
- 稿件说明：
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吴翠, 马玉翠, 洪专, 等. 4种根茎类中药材在简易库和冷藏库中的理化指标分析[J]. 中国实验方剂学杂志, 2018,24(8):60-64.

WU Cui, MA Yu-cui, HONG Zhuan, et al. Analysis on Physiochemical Indexes of Four Kinds of Rhizome Chinese Medicinal Herbs Stored in Simple and Cool Warehouses[J]. Chinese journal of experimental traditional medical formulae, 2018, 24(8): 60-64.
吴翠, 马玉翠, 洪专, 等. 4种根茎类中药材在简易库和冷藏库中的理化指标分析[J]. 中国实验方剂学杂志, 2018,24(8):60-64. DOI： 10.13422/j.cnki.syfjx.20180808.

WU Cui, MA Yu-cui, HONG Zhuan, et al. Analysis on Physiochemical Indexes of Four Kinds of Rhizome Chinese Medicinal Herbs Stored in Simple and Cool Warehouses[J]. Chinese journal of experimental traditional medical formulae, 2018, 24(8): 60-64. DOI： 10.13422/j.cnki.syfjx.20180808.

摘要

目的：探究何首乌、白芷、三七、三七粉4种根茎类中药材在2种贮藏条件下外观及化学成分随贮藏时间的变化规律。方法：这4种中药材分别置于简易库和冷藏库中贮藏27或33个月。日光下观察药材的色泽。烘干法测定水分。高效液相色谱法测定化学成分的含量。结果：随着贮藏时间的延长，简易库和冷藏库中何首乌的色泽均逐渐加深，5-羟甲基糠醛的含量呈波动升高趋势；简易库中何首乌的二苯乙烯苷含量呈波动下降趋势，结合蒽醌含量呈波动升高趋势；冷藏库中二苯乙烯苷含量呈波动升高趋势，结合蒽醌含量变化不明显。两库中，白芷的色泽均逐渐加深，欧前胡素含量均未见明显变化；三七和三七粉的色泽，人参皂苷Rg1，Rb1及三七皂苷R1的含量均未见明显变化。结论：何首乌经33个月，白芷、三七、三七粉经27个月的贮藏，无论是简易库还是冷藏库，尽管发生了色泽和化学成分含量的轻度变化，但均在合格药材的质量标准范围内。

Abstract

Objective: To explore the change rules of color and chemical components of four kinds of rhizome Chinese medicinal herbs[Polygoni Multiflori Radix(PMR)

Angelicae Dahuricae Radix(ADR)

Notoginseng Radix et Rhizom

powder of Notoginseng Radix et Rhizoma] under two kinds of storage conditions. Method: These Chinese medicinal herbs were stored in simple warehouse and cool warehouse for 27 or 33 months. Their color was then observed under the sunlight. Their water content was determined based on the drying method. The contents of chemical components were determined by high performance liquid chromatography (HPLC) method. Result: With the increase of storage time

the color was deepened gradually and the content of 5-hydroxymethylfurfural (5-HMF) was increased in a wavy way for PMR stored in simple warehouse and cool warehouse. The content of stilbene glycoside was decreased and the content of combined anthraquinones was increased in a wavy way for PMR stored in simple warehouse. The content of stilbene glycoside was increased in a wavy way and the content of combined anthraquinones had no significant change for PMR stored in cool warehouse. The color deepened gradually and the content of imperatorin had no significant change for ADR stored in both simple warehouse and cool warehouse. The contents of ginsenosides Rg1 and Rb1 and notoginsenoside R1 as well as the color of Notoginseng Radix et R hizoma (NRR) and powder of Notoginseng Radix et Rhizoma showed no significant changes. Conclusion: The color and the contents of chemical components in PMR after 33 months and ADR

NRR and powder of NRR after 27 months storage in both simple warehouse and cool warehouse were changed slightly

but the quality of these four rhizome Chinese medicinal herbs were still controlled within the standard range.

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