泛油对千金子主要有效成分含量的影响

张宏伟; 金锋; 张振凌

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泛油对千金子主要有效成分含量的影响

更新时间：2024-01-04

- 泛油对千金子主要有效成分含量的影响
- Impact of Oil-releasing to Content of Main Effective Components of Semen Euphorbiae
- 中国实验方剂学杂志 2012年18卷第22期页码：124-126
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  中医药行业科研专项子项目(201107008)
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- 纸质出版日期：2012
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张宏伟, 金锋, 张振凌. 泛油对千金子主要有效成分含量的影响[J]. 中国实验方剂学杂志, 2012,18(22):124-126.

ZHANG Hong-wei, JIN Feng, ZHANG Zhen-ling. Impact of Oil-releasing to Content of Main Effective Components of Semen Euphorbiae[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(22): 124-126.
张宏伟, 金锋, 张振凌. 泛油对千金子主要有效成分含量的影响[J]. 中国实验方剂学杂志, 2012,18(22):124-126. DOI：

ZHANG Hong-wei, JIN Feng, ZHANG Zhen-ling. Impact of Oil-releasing to Content of Main Effective Components of Semen Euphorbiae[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(22): 124-126. DOI：

摘要

目的: 比较泛油对千金子种仁中脂肪油及千金子甾醇的含量的影响。方法: 索式提取法提取脂肪油并测定含量;高效液相色谱法测定千金子甾醇含量

Agilent Rx-SIL液相色谱柱(4.6 mm×250 mm

5 μm)

流动相正己烷-乙酸乙酯-乙腈(87.5∶10∶2.5)

柱温30 ℃

检测波长275 nm

体积流量1.0 mL·min-1。结果: 未泛油千金子种仁脂肪油平均含量为62.48%

千金子甾醇平均含量为1.20%;泛油千金子种仁脂肪油平均含量为53.66%

千金子甾醇平均含量为1.10%。结论: 千金子种仁泛油后其脂肪油及千金子甾醇含量均降低。

Abstract

Objective:Compare the content of the fat oil and the euphorbia factor L1 of semen euphorbiae seed kernel before and after oil-releasing. Method: Soxhlet extraction was used to extract the fat oil and determine content. The content of euphorbia factor L1 were determined by HPLC. An Agilent rx-sil column (4.6 mm×250 mm

5 μm) was used with normal hexane-ethyl acetate-acetonitrile (87.5∶10∶2.5) as the mobile phase

the flow velocity was at 1.0 mL·min-1

UV detection was at 275 nm and temperature was at 30 ℃. Result: The content of the fat oil and the euphorbia factor L1 of normal semen euphorbiae seed kernel were 62.48% and 1.20%. The content of the fat oil and the euphorbia factor L1 of oil-releasing semen euphorbiae seed kernel was 53.66% and 1.10%. Conclusion: The content of the fat oil and the euphorbia factor L1 of oil-releasing semen euphorbiae seed kernel was reduced.

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