八宝惊风散的定性定量方法

唐丽丽; 何绍萍; 陈华龙

doi:10.11653/syfj2013190146

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八宝惊风散的定性定量方法

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- 八宝惊风散的定性定量方法
- Studies on the Qualitative and Quantitative Methods of Babao Jingfeng San
- 中国实验方剂学杂志 2013年19卷第19期页码：146-148
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- DOI：10.11653/syfj2013190146
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- 纸质出版日期：2013
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唐丽丽, 何绍萍, 陈华龙. 八宝惊风散的定性定量方法[J]. 中国实验方剂学杂志, 2013,19(19):146-148.

TANG Li-li, HE Shao-ping, CHEN Hua-long. Studies on the Qualitative and Quantitative Methods of Babao Jingfeng San[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(19): 146-148.
唐丽丽, 何绍萍, 陈华龙. 八宝惊风散的定性定量方法[J]. 中国实验方剂学杂志, 2013,19(19):146-148. DOI： 10.11653/syfj2013190146.

TANG Li-li, HE Shao-ping, CHEN Hua-long. Studies on the Qualitative and Quantitative Methods of Babao Jingfeng San[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(19): 146-148. DOI： 10.11653/syfj2013190146.

摘要

目的: 建立八宝惊风散的定性定量方法。方法: 采用气相色谱法对八宝惊风散中人工麝香进行定性鉴别

采用气相色谱测定制剂中丁香和冰片的含量。采用SUPELCO SUPELCOWAXTM-10石英毛细管色谱柱

梯度升温

进样口温度175℃;检测器温度240℃。结果: 在气相色谱中能检出人工麝香;含量测定中丁香酚在0.020 12~0.100 6 μg呈良好的线性关系(r=0.999 3);龙脑在0.080 33~0.401 65 μg呈良好的线性关系(r=0.999 1)。结论: 建立的分析方法简便可行

专属性强

可用于八宝惊风散的定性定量检测。

Abstract

Objective: To study the qualitative and quantitative methods of Babao Jingfeng San. Method: Artificial muskin Babao Jingfeng San were identified with the method of GC

The contents of Eugenol and Borneol were determined with the method of GC. Using SUPELCO SUPELCOWAXTM-10 quartz capillary column

gradient temperature

inlet temperature: 175℃

detector temperature: 240℃。Result: In GC

Artificial musk can be detected and without interference. Quantitative analysis of GC showed that the linear ranges of Eugenol and Borneol were 0.020 12-0.100 6 μg (r=0.999 3) and 0.080 33-0.401 65 μg

(r=0.999 1)

respectively. Conclusion: The methods set up by this study are accurate and easy to perform with the merits of good resolution

specificity and reproducibility. It can be used for the qualitative and quantitative detection of Babaojingfeng San.

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