GC-MS分析羌药关节炎散挥发油化学成分

盛菲亚; 傅超美; 胡慧玲; 林俊芝; 李莹; 包希福

doi:10.11653/syfj2014010087

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GC-MS分析羌药关节炎散挥发油化学成分

更新时间：2024-01-04

- GC-MS分析羌药关节炎散挥发油化学成分
- Chemical Constituents Analysis of Volatile Oil in Arthritis Powder of Qiang Medicine by GC-MS
- 中国实验方剂学杂志 2014年20卷第1期页码：87-90
- 作者机构：
- 作者简介：
- 基金信息：
  
  四川省科技厅科技支撑计划项目（2011SZ0063）
- DOI：10.11653/syfj2014010087
  中图分类号：
- 纸质出版日期：2014
- 稿件说明：
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盛菲亚, 傅超美, 胡慧玲, 等. GC-MS分析羌药关节炎散挥发油化学成分[J]. 中国实验方剂学杂志, 2014,20(1):87-90.

SHENG Fei-ya, FU Chao-mei, HU Hui-ling, et al. Chemical Constituents Analysis of Volatile Oil in Arthritis Powder of Qiang Medicine by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(1): 87-90.
盛菲亚, 傅超美, 胡慧玲, 等. GC-MS分析羌药关节炎散挥发油化学成分[J]. 中国实验方剂学杂志, 2014,20(1):87-90. DOI： 10.11653/syfj2014010087.

SHENG Fei-ya, FU Chao-mei, HU Hui-ling, et al. Chemical Constituents Analysis of Volatile Oil in Arthritis Powder of Qiang Medicine by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(1): 87-90. DOI： 10.11653/syfj2014010087.

摘要

目的：用气相色谱-质谱联用（GC-MS）技术分离鉴定羌药关节炎散挥发油的化学成分。方法：水蒸气蒸馏法提取关节炎散挥发油，采用GC-MS法分离鉴定，用面积归一法测定各化合物相对含量。结果：共分离鉴定了33个化学成分，占总成分相对含量的86.47%，其中相对含量超过5%的成分有丹皮酚（13.20%）、芳樟醇（10.94%）、白菖烯（9.48%）、枞油烯（7.93%）、2-亚甲基-6，8，8，-三甲基-三环[5.2.2.0（1，6）]十一碳-3-醇（5.01%）。结论：可为关节炎散的质量控制和进一步药效研究提供一定的参考。

Abstract

Objective: To analyze the chemical constituents of the volatile oil from arthritis powder of Qiang medicine by GC-MS. Method: The water distillation was used to extract the volatile oil

GC-MS technology was used to analyze the components of the volatile oil

and area normalization was used to determine the relative content of each component. Result: Thirty-three chemical components were identified

which was 86.47% of total components. The relative amounts of 5 components were above 5%. They were paeonol (13.20%)

linalool (10.94%)

(+)-calarene (9.48%)

sylvestrene (7.93%)

tricyclo [5.2.2.0(1

6)] undecan-3-ol

2-methylene-6

8-trimethyl-(5.01%). Conclusion: The experiment provides some evidence of quality control and further pharmacodynamics study foundation of arthritis powder.

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